Categories
Combustion Analyzer Tips & Tricks

Graphite on the CS1232 Carbon Analyser

[vc_row][vc_column width=”1/4″][vc_single_image image=”796″ img_size=”full”][/vc_column][vc_column width=”3/4″][vc_custom_heading text=”Configuring the Method” font_container=”tag:h3|text_align:left|color:%230055a5″ use_theme_fonts=”yes”][vc_column_text]To accurately achieve the desired results as shown in the table below, the method if the CS1232 Carbon Sulphur analyser first needs to be configured correctly.

  1. Set your lance delay time to the maximum time of the sample. This effectively turns off the lance purge. This needs to be done to prevent saturation of the Carbon IR cell. This happens because Carbon will be released from the sample very quickly.
  2. Set your maximum time to 600 seconds. This is to make allowances for the sample mass being used. The software will stop the analysis according to the end of analysis settings that are set.
  3. Set the baseline offset voltage to 50mV. As the Carbon concentration for Graphite is typically above 60%, you need to ensure that the settings used here is suitable for your instrument.
  4. Set the baseline end time (the time required that the sample must meet the stability settings for it to be deemed “stable” before the end of analysis is computed) to 15 seconds.
  5. Set the baseline stability (the allowable value that can vary from the computed/current baseline valve) to 15mV. This settings works in conjunction with step 4 above.

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It is very important to keep everything as clean as possible. This means all weighing utensils, the balance pan and the workspace else the weighed crucible could pick up fine graphite particles that will bias the result. It is also very important that any air conditioning or air flows within the lab are not directed at the weighing work area. This is because graphite is extremely light in mass and will easily be blown about the work area contaminating it.

[/vc_column_text][/vc_column][/vc_row][vc_row full_width=”stretch_row” css=”.vc_custom_1606751003353{background-image: url(https://labfit.com/wp-content/uploads/2020/11/product-list-banner.jpg?id=494) !important;}”][vc_column][vc_custom_heading text=”Balance enclosures” font_container=”tag:h3|text_align:center|color:%230055a5″ use_theme_fonts=”yes”][vc_column_text]

Add a balance enclosure to your lab. They are great for weighing very light samples and prevent the sample from being subjected to air flows within the lab caused by air conditioning systems/ventilation.

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Once the samples have been weighed, place the sample carousel into the CS1232 Carbon Sulphur analyser. Make sure that the furnace is at temperature 1350-1400° C. You can run the analyser at a lower temperature but the this will extend the analysis time. The temperature stated is the normal operating temperature that will allow you to measure Sulphur species as well.

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Categories
Combustion Analyzer

Graphitic Carbon Analysis

[vc_row][vc_column][vc_custom_heading text=”CS1232 Carbon Analyser 95% Graphite” font_container=”tag:h3|text_align:left|color:%230055a5″ use_theme_fonts=”yes”][vc_column_text]

The CS1232 Carbon and Sulphur Analyser successfully tested 95% graphite using a representative sample mass of 0.2 gram. The tested samples were of unknown origin but had an expected value from an LOI test. Graphite is extremely light weight and therefore it is important to note that you must at all times keep the work space 100% spotless.

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Categories
Combustion Analyzer

What is elemental analysis and how is it used in soil testing?

[vc_row][vc_column][vc_column_text]The elemental analysis is the most profound method for identifying the basic or potentially isotopic characteristics of gases, fluids, or solids. This method is carried out with the help of an automated and preprogrammed analyzer that tests specific contaminants as well as components.

When a component is examined for its basic properties it is known as Elemental Analysis and is performed with the help of elemental analyzer. This is a procedure which utilizes a specimen of material, and this sample is examined for its basic and frequent isotopic organization.

By utilizing this procedure, the components which are available can be resolved; this is known as ‘qualitative’, and the procedure could be helpful to decide the amount of every component that is its ‘quantitative’ value.

Today, the basic analyzers are ordinarily used for ecological examination, with an accentuation on shielding the normal and human conditions from mechanical waste. To finish this objective, researchers use a diverse range of essential analyzers tests in order to know the[/vc_column_text][vc_column_text]

  • Greenhouse gas emissions
  • Particulate emissions
  • Source gas emissions
  • Ambient gas emissions

[/vc_column_text][/vc_column][/vc_row][vc_row][vc_column][vc_custom_heading text=”Elemental analysis for soil testing” font_container=”tag:h3|text_align:left|color:%230055a5″ use_theme_fonts=”yes”][vc_column_text]The soil is one of the most essential carbonic elements with various chemical and organic properties. Soil analysis focuses on testing the agricultural soil for contamination and its fertility. It is also conducted to understand the fact that how certain disposed solids affect soil in the long-term and testing commercial and industrial sites for contaminant buildup. To perform these tests, private organizations and government agencies use a wide range of equipment and machines. Some of the popular equipment used for elemental testing of soil is Spectrometers, Autosamplers, Microanalysis & electron microscopy systems and dissolved oxygen meters.

Scientists and soil experts use essential investigation prior conducting this test on soil such as CHNX examination. The data extracted from the elemental test is vital in knowing the structures of the different elements in the soil which is very important to decide the fertility of the soil.[/vc_column_text][/vc_column][/vc_row]